日本質量分析学会 第67回質量分析総合討論会

演題概要

ポスター発表

第2日 5月16日(木)  P会場(多目的ホール)

モノクロロプロパンジオールモノエステルの順相LC-MS/MS定量分析

(大阪産業技術研)
o佐藤博文渡辺嘉靜間基博

The qualification and quantification of monochloropropanediol (MCPD) monoesters were achieved by normal phase liquid chromatography utilizing C60 column coupled with tandem mass spectrometry (LC-MSMS). MCPD monoesters which have fatty acyl group were separated without overlap prior to MS/MS within 15 min and were accurately quantified. Moreover, even peak-overlapped 3-MCPD-monoesters in chromatogram could be also quantified applying multiple reaction monitoring (MRM).