The 45th Annual Conference
on Mass Spectrometry, Nara, 1997

May 14th-16th, 1997
Nara Women's University, NARA (Japan)

[Program in Japanese] [The 45th Annual Conference on Mass Spectrometry]
[Dr. T. Takeuchi] [Staffs] [Department of Chemistry]


PROGRAM



Wednesday, May 14th, 1997



[Oral Session]


(9:30-10:50)

Chair: K. Shiratsuchi
1-O-1
Space Charge Effect in the Ion Beam Design and the Optimization of Sector Magnet for High Current Ion Beam
(ULVAC JAPAN Ltd.) *O.Tsukakoshi , K.Niikura , T.Terasawa

1-O-2
Precise Design of Shims with large Gap by Computer Simulation
(ULVAC JAPAN Ltd.) *O.Tsukakoshi , K.Niikura , T.Terasawa

1-O-3
(JEOL) *Y. Takahashi, K. Matsuura, I. Nijima

1-O-4
Sonic Spray Ionization for Liquid Chromatography/Mass Spectrometry
(Central Research Laboratory , Hitachi , Ltd.)
*Y.Hirabayashi , A.Hirabayashi , Y.Takada , M.Sakairi , H.Koizumi


(10:50-11:50)

Chair: A. Hirabayashi
1-O-5
Basic study of Electrospray Ionization method (3)
(Nohmi Bosai Co.Ltd.) *Takashi Nohmi , Maya Maekawa , J.B.Fenn

1-O-6
Structural Analysis by Detecting Post Source Generated Neutral Species
(Analytical Instruments Div., Shimadzu Corp.)
*Shin-ichiro Kawabata , Koichi Tanaka

1-O-7
Development of Highly Sensitive Interfaces for LC/3DQMS
(Central Research Laboratory , Hitachi , Ltd.)
*Y.Takada and M.Sakairi


[Poster Session]


(13:00-15:00)

1-P-01
The Study of Molecular Weight Distribution Measurement for Macromolecules Using SIMS
---Methyl Methacrylate Oligomer System---
(Nara Women's Univ., Kobe Pharmaceutical Univ.)
*K.Momoji , I.Miyamoto , T.Takeuchi , K.Iwai , M.Yamamoto and K.Saiki

1-P-02
Differences of cations and anions in ion-solid interactions
(Osaka National Research Institute , Nara Women's Univ.)
*M.Kiuchi , T.Takeuchi , M.Yamamoto

1-P-03
Analysis of Peak Coalescence Phenomenon in FT-ICR Mass Spectrometry Using Massively Parallel Computers
(Univ.Electro-Communications , Hiroshima City Univ.)
*A.Uemura , M.Fujiwara , M.Inoue

1-P-04
Comparison of FAB, APCI and ESI Spectra for Non-volatile Compounds
(JEOL LTD.) *K.Matsuura , Y.Takahashi , and K.Nojima

1-P-05
Vibronic excitation of molecules by ion impact
(Osaka Prefecture Univ.)
*K.Iwamoto , K.Yamamoto , A.Matsumoto

1-P-06
Interaction between sugar and ethanol in aqueous ethanol solution studied by liquid ionization mass spectrometry
(Yokohama National Univ., Takara Brewery Ltd.)
*Yokoyama,Y., Nagahara,H., Inoue,T., Tsuchiya,M.

1-P-07
Electrospray LC/MS Analysis using CrossFlow Counter Electrode
(Jasco International Co., LTD)
*N.Kagi , S.Furusho , A.Shibata

1-P-08
A challenge to the "Supramolecular Chemistry" by means of Mass spectrometry
Mass-spectrum of Macrocyclic Pd(II) Complex (3)
(Analysis Center, Faculty of Engineering, Faculty of Science, Chiba Univ. , Pharmaceutical,Meijyoh Univ., Thermo Quest K.K.)
*T.Kuramochi , K.Masuda , M.Kanai , M.Fujita , K.Ogura, M.Funabashi , K.Yamada , M.Yokoyama

1-P-09
Metastable decomposition of alkyl fluoroacetates
(Gunma National College of Technology)
*Osamu Sekiguchi , Risei Koitabashi and Susumu Tajima

1-P-10
The routes of formation and decomposition of the m/z 59 ions with elemental composition C3H7O generated upon electron impact of methyl propanoate
(Gunma National College of Technology, Hoshi College of Parmacy, University of Amsterdam)
K.Aoyagi, *M.Fujishige , O.Sekiguchi, S.Tajima , A.Shigihara , N.M.M.Nibbering

1-P-11
Structural Analysis of Photo-oxidized (Ethylenediamine)bis(2,2'-bipyridine) ruthenium(II) Complexes Using On-Ione ES-MS of Labeled Compounds
(Department of Applied Chemistry, Osaka University, Department of Physics , Osaka University)
*F.Matsuda , G.Matsubayashi , T.Matsuo , R.Arakawa

1-P-12
Mass Spectra of CrO(TPP) Complexes
(Aichi Kyoiku Univ., Meijo Univ.)
T.Tunoda , T.Miyake , M.Kaneko, *H.Konishi , M.Inamo , N.Takeda , H.Yosizumi , A.Tatematu

1-P-13
ES-MS Analysis of Metal-Ion Complexation Photocontrol for Azacrowned Malachite Green
(Dept. of Chemistry, Osaka City University, Dept. of Applied Chemistry, Osaka University, Dept. of Physics, Osaka University)
*M.Okamoto , K.Kimura , M.Yokoyama , H.Doe, T.Matsuo , R.Arakawa

1-P-14
Selective Complexes of a New Family of Cyclic Oligosaccharide Hosts with Metallic Cation Guests in Electrospray Ionization Mass Spectrometry
(Osaka Municipal Technical Resarch Institute , Fuzisawa Pharm.Co.Ltd., MAC , ISIR, Osaka Univ.,Department of Biology, Osaka Kyouiku Univ.)
*Shizuma, M.; Totsuka, Z.; Matsuda, K.; Yamato, Y.;Takai, Y.; Uchiyama, T. ;Takeda, T. ;Sawada, M.

1-P-15
Chiral Amino Acid Recognition of Mono-, Di-, and Tri-Saccharide Derivatives detected by FAB Mass Spectrometry
(ISIR, Osaka Univ., Osaka Municipal Inst.)
M.Sawada, *H.Yamada , M.Shizuma , Y.Takai , T.Takeda

1-P-16
Chiral Molecular Recognition of Chiral Crown Host in Electrospray Ionization Mass Spectrometry
(MAC, ISIR, Osaka Univ. , Osaka Women's Univ. , Faculty of Engineering, Osaka Univ., Faculty of Science, Osaka Univ.)
*Y.Takai , H.Yamaoka , H.Horiguchi , R.Arakawa, G.Matsubayashi , T.Matsuo , M.Sawada

1-P-17
Liquid Matrix-Assisted Laser Desorption/Ionization Tandem Mass Spectrometry: Evaluation of LMALDI High Energy CID Spectrum
(Suntory Institute for Bioorganic Research)
*T.Fujita , Y.Itagaki , M.Hisada , H.Naoki , T.Nakajima

1-P-18
Attempts of B/E Linked Scanning Technique from Multiply Charged Ions by Magnetic Sector Mass Spectrometry(2)
(Meijo Univ., JEOL DATUM Ltd., JEOL Ltd.)
*Katsuyoshi Masuda , Toyohiro Haramo , Kazutetsu Nojima

1-P-19
CID Spectra of protonated dimer ions of dipeptides by means of ESI-QQQ Mass Spectrometry
(Fac.of Technology, Fukui Univ., Fukui Medical School, Fac.of Education, Fukui University)
K.Oyya , S.Tanaka, *M.Yoshimura , K.Isa

1-P-20
Analysis of MALDI by inorganic matrix
- The application of various low molecule organic compounds -
(Nippon Roche Research Center, Shimadzu)
*Y.Nakamura , Y.Fujimoto , N.Nakayama , K.Tanaka , S.Kawabata

1-P-21
Unimolecular Dissociation for N-(Substitutedphenylacetyl)azacycloalkan-2-thione Derivatives: Comparison with the Corresponding Azacycloalkan-2-one System
(Department of Natural Science, Osaka Women's University)
*Yamaoka, Hirashi; Takagi, Nana

1-P-22
Labile parts of O-acyl oximes and its structure
(Mukogawa Women's Univ., Toho Univ.)
*S.Horiyama , K.Suwa, M.Yamaki , H.Kataoka , T.Katagi , M.Takayama

1-P-23
Study of Dendritic Macromolecules by MALDI-TOFMS
(Communications Research Laboratory)
*S.Yokoyama , S.Mashiko

1-P-24
Structural charactarization of silicone polymer by MALDI-TOF
(Shiseido safety & analytical research center)
*S.Yoshida , S.Yamamoto , T.Takamatsu

1-P-25
High Performance Liquid Chromatography (Photodiode array detector)/Atmospheric Pressure Chemical Ionization Mass Spectrometry of Carotenoids
(Kyoto Pharmaceutical University, Research Institute for Production Development)
K.Hashimoto, *T.Maoka , Y.Fujiwara

1-P-26
FAB Mass Spectra of Methamphetamine Hydrochloride
(Fukui Pref. Police H.Q., Fukui Univ.)
*S.Matsumura , F.Masuyama, R.Tsukamoyo , K.Isa

1-P-27
Structural Determination of New Polyisoprenepolyols Isolated from an Edible Mushroom by Fast Atom Bombardment Mass Spectrometry
(Kinki Univ.ICAS , Kinki Univ.JRC , Kinki Univ.FA)
A. Sawabe, *M. Moritai, S. Ouchi, and T. Okamoto

1-P-28
Simultaneous Determination of Menaquinone-4 and Its Metabolite in Human Osteoblasts by High-Performance Liquid Chromatography/Atmospheric Pressure Chemical Ionization Tandem Mass Spectrometry
(Eisai Co., Ltd., Tokyo Metropolitan Institute of Gerontology)
*Y.Sano , K.Kikuchi , K.Tadano , K.Hoshi , Y.Koshihara

1-P-29
Development of sensitive derivatization reagent for thiol group in LC-MS analysis
(Santen Pharmaceutical) *Kenji Matsuura , Hideo Takashina

1-P-30
FAB Mass Spectrometry of Metalloporphyrin Related Compounds with Tumor Tissue Affinities
(Faculty of Pharmacy, Meijo Univ., Fculty of Integrated Arts and Sciences, Aichi Kyoiku Univ., Toyo Hakka Kogyo Co., Ltd.)
*N.Takeda , H.Yoshizumi , H.Ohshima , H.Konishi , I.Sakata

1-P-31
Determination of Absolute Configuration of Primary Amino Compounds Including Amino Acids Using LC/MS
(Faculty of Pharmacy, Meijo University, Aichi Prefectural Institute of Public Health)
*K.Fujii , T.Shimoya , M.Suzuki , K.-I.Harada, Y.Ikai , H.Oka

1-P-32
Development of Mass separated, ultra high vacuum, very low energy ion beam irradiation and ion beam deposition systems
(ULVAC JAPAN Ltd.) *O.Tsukakoshi

1-P-33
Charged Droplet Formation in Sonic Spray
(Central Research Laboratory , Hitachi , Ltd., Yale Univ.)
*A.Hirabayashi , J.F.de la Mora


[WORKSHOP]

(15:00-18:00)

Chairs: H. Miyata, T. Fujii (W-1)

W-1
Recent Counterplan and Problems for Pollution by Dioxin and Analogues

1-1 Real Situation and Problems Associated with the Analysis of DIOXIN

1-2 Real Situation and Problems of Environmental Pollution

1-3 Real Situation and Problems of law and regulation


(15:00-18:00)
Chair: H. Naoki (W-2)

W-2
A Role of Mass Spectrometry in Molecular Biology

2-1 A Role of Mass Spectrometry in Molecular Biology

2-2 Automated Interpretation of MS/MS Spectra by "SeqMS",a Software Aid for Peptide

2-3 On a research experience from Prof.Catherine Fenselau's lab.

2-4 Ultra-high sensitive ESIMS analysis and its application to the identification of mutant proteins in blood

2-5 From Structural Analysis of Natural Products to Molecular Biology via Biological Mass Spectrometry

[Exhibition] 9:30-17:00



Thurday, May 15th, 1997



[Oral Session]


(9:00-10:00)

Chair: K. Hiraoka


2-O-01
Two Dimentional Detection of Elastic and Inelastic Process in CID
(Osaka Univ.) *M.Arimura , G.Matubayasi

2-O-02
Structural Studies on Scandium Endohedral Metallofullerenes by a High Resolution Gas Ion Chromatography
(Department of Chemistry, Nagoya University, Department of Chemistry, Northwestern University)
*Toshiki Sugai, Masayasu Inakuma , Hisanori Shinohara , Robert Hudgins, Philippe Dugourd , Martin Jarrold

2-O-03
Collison between Noble Atom and Fullerene at a few KeV
(Inst.of Physics Univ.of Tsukuba, Upjohn & Pharmaceusticals Ltd. Stractual Chemical Group)
*T.Kurita , S.Tomita, T.Nishimura , S.M.Lee


(10:00-11:00)

Chair: M. Arimura


2-O-04
The Characteristic Structures of Cluster Ions F(-)(M)n, M=O2,N2,CO,and CO2
(Faculty of Engineering , Yamanashi University)
*T.Sugiyama , J.Katsuragawa , K.Hiraoka

2-O-05
Effect on the dissolution of silica by alkaline, alkaline earth ions; study of the chemical form in the solution using FAB-MASS
(The Tokyo University of Fisheries, The Institute of Physical and Chemical Research (RIKEN))
*Miho Tanaka and Kazuya Takahashi

2-O-06
The Ion-Stimulated Desorption of Van der Waals Thin Films Induced by Low-Energy Ion Impact: Time Domain of Secondary Ion Formation
(Yamanashi Univ.) *T.Sato, R.Hamamoto, K.Hiraoka


(11:00-12:00)
Chair: I. Katakuse
Plenary Lecture
In-situ isotopic Analyses of Solid Geochemical Samples using Laser Ablation-Multiple Collector-Inductively Coupled Plasma Mass Spectrometry
(Tokyo Institute of Technology) Hirata, T.


(13:00-14:20)
Chair: M. Yamawaki
SHOUREI Award Lecture
Unimolecular Dissociation of Gaseous Ions in EI Mass Spectrometry
(Nara Women's University) Takae Takeuchi

SHOUREI Award Lecture
Development of High Performance Time-of-Flight Mass Spectrometer Consisting of Four Electrostatic Sector Analyzers
(Japan Advanced Institute of Science and Technology) Toru Sakurai

GAKKAI Award Lecture
Development and Application of Liquid Ionization Mass Spectrometry
(Yokohama National University) Tsuchiya,M.

GAKKAI Award Lecture
Development of High Performance Mass Spectrometer
(Emeritus Professor,Osaka Univ.) H.Matsuda



[Oral Session]


(14:20-15:40)

Chair: M. Asano
2-O-07
Development of a TOF type neutral gas mass spectrometer for spacecraft measurement
(Institute of Space and Astronautical Science)
*N.Fujikawa , K.Tsuruda , H.Hayakawa , S.Abe

2-O-08
Development of a system to control the atmosphere gas pressure and composition in Knudsen cell
(Univ.of Tokyo)
*M.Yasumoto , M.Tonegawa , A.Suzuki , J.Huang, and M.Yamawaki

2-O-09
Vaporization Properties of Cesium Uranate with and without Addition of D2 or D2O
(Univ.of Tokyo, Nippon Nuclear Fuel Development Co.Ltd.)
*J.Huang, M.Yamawaki, M. Yasumoto, K.Yamaguchi and H.Sakurai

2-O-10
Study on vaporization behavior of Li2TiO3 by means of atmosphere controllable high temperature mass spectrometry
(Faculty of Engineering, The Univ.of Tokyo, Research Center for Nuclear Science and Technology, The Univ.of Tokyo)
M.Yamawaki, *A.Suzuki , M.Tonegawa , M.Yasumoto , K.Yamaguchi



[Poster Session]


(15:40-17:40)

2-P-01
Fragmentation appeared in CAD spectra of protonated urea-relatives and FAB MS spectra of mixtures of alkali metal chlorides and matrices
(Faculty of Education, Fukui University)
*R.Tsukamoto , K.Isa, and M.Yamamoto

2-P-02
Structural Analysis of Glycoprotein in Human Urine using Semi-micro LC/FAB-MS Technique
(Shiseido Co. Pharmaceutical Research Laboratories, Thrombosis Chemical Institute)
*A.Motoyama , K.Ogino , T.Matsumoto, H.Shimada , J.Kikuchi , R.Namba , S.Hayashi

2-P-03
FAB-MS/MS and ESI-MS/MS of Peptides on a Four Sector Tandem Mass Spectrometer
(Sumitomo Chemical) *T.Mikami , K.Yanagi , H.Nakazawa

2-P-04
Investigation of the complex formation between lectins and metal ions or sugars by MALDI-TOF mass spectrometry
(National Food Research Institute, Shizuoka Univ.)
*M.Kameyama-O. , T.Nagata , H.Nakamura , H.Kawagishi

2-P-05
Mass spectrometry of sulfated glycoglycerolipids Structural characterization by MALDI-TOFMS and LSIMS
(Department of Biochemistry , Teikyo Univ. School of Medicine, Tokyo CSC , Shimadzu Corp.)
*K.Tadano-Aritomi , S.Kawabata , N.Iida-Tanaka , I.Ishizuka

2-P-06
Mass Spectra of Macrolide Antibiotics-II
- FAB and SIMS of Qudrupole and Magnetic Sector Type Mass Spectrometry-
(Tokyo Univ.of Pharm.& Life Science, Chiba Univ., The Univ.of Tokyo, Tokyo Medical and Dental Univ.)
*Y.Shida , M.Fukuzawa , K.Ohara , T.Sawai , T.Takahashi , T.Kasama

2-P-07
Structural elucidation of novel components as CYP3A4 P450 inhibitors in Grapefruit Juice
(Pharm.Res.Lab., Tanabe Seiyaku Co.Ltd. and Pharm.Tohoku Univ.)
*N.Ohashi , K.Fukuda , S.Furuuchi , M.Yoshikawa , T.Ohta , Y.Yamazoe

2-P-08
Identification of rat urinary main metabolite of new aldose reductase inhibitor AS-3201
(Developmental Research Laboratories , Discovery Research Laboratories I, Dainippon Pharmaceutical Co.)
*H.Toda , K.Toide , A.Itogawa , H.Matsushita , Y.Terauchi , T.Hujii

2-P-09
Optimization of Experimental Conditions in MALDI-TOF MS, and Application to Structural Analysis of Unsequenced Protein
(Analytical and Metabolic Research Laboratories, Sankyo Co., Ltd.)
*T.Kosaka , T.Takazawa , T.Nakamura

2-P-10
Animicrobial Activity of Calopyllum blancoi Pl. et Tr. in Philippines
(Kobe Pharmaceutical Univ. University of Illinois at Chicago, National Museum, Manila)
*K.Kawanishi, K.Saiki , H.Nanba , Doel D.Soejarto , Domingo A.Madulid

2-P-11
Structural Determination of Peptide Compounds Produced by Cyanobacteria Using MS/MS Method
(Faculty of Pharmacy, Meijo University, Central Research Laboratories, Ajinomoto Co.Inc., Marine Biotechnology Institute Co.,Ltd, Department of Applied Chemistry and Microbiology, University of Helsinki,Helsinki)
*K.Fujii , M.Suzuki , K.-I.Harada , K.Noguchi , K.Hirayama , K.Adachi, H.Sano , K.Sivonen

2-P-12
Analysis of Wasp Toxin Peptides using Enzymatic Ladder Sequencing and MALDI-TOF-CID methods
(SUNBOR, Teikyo Univ.)
*M.Hisada , Y.Itagaki , H.Naoki , T.Nakajima , K.Konno , H.Takayama

2-P-13
To establish the position of disulfide linkages in peptidyl spider toxins with the advantages that are high mass sensitivity and easy handling
(Suntory Institute for Bioorganic Research, University of Frankfult)
*A.Yasuda , M.Hisada , T.Fujita , Y.Itagaki , H.Naoki , T.Nakajima, D.Mebs

2-P-14
Structural Elucidation of Fatty Acid Components of Liposidomycins by MS/MS/MS Method
(RIKEN, Snow Brand Milk Products Co.,Ltd., JEOL DATUM, Tamagawa Univ.)
*Y.Esumi , Y.Suzuki , K.Kimura , M.Yoshihama , T.Ichikawa , M.Uramoto

2-P-15
Mass Spectrum of Coconut Oil Precipitate
(Kanagawa Univ., Yokohama National Univ.)
*Y. Mochida , S. Nakamura , M. Tsuchiya

2-P-16
Odor analysis of polymer samples during thermal decomposition
(Nohmi Bosai LTD.,Seikei Univ.)
*M. Maekawa , T. Nohmi , T. Inoue , A. Higuchi

2-P-17
Metastable Decomposition of TMS-CH2OH, TMS-CH2SH, TMS-OCH3 and TMS-SCH3 upon Electron Impact
(Gunma National College of Technology , Shin-Etsu Chemical Co.Ltd , Sankyo Co.Ltd , Hoshi College of Parmacy)
O.Sekiguchi , *S. Tajima, S.Mori , T. Kinoshita , A. Shigihara

2-P-18
Ion/Molecule Reactions of Silene Radical Cations with Alkene Molecules in FT-ICR Mass Spectrometry
(Nara Women's Univ. , Univ. of Amsterdam)
*Takae Takeuchi , Masao Yamamoto , Roel H. Fokkens , Nico M. M. Nibbering

2-P-19
Analysis of Biological and Environmental Compounds Using LC/3DQMS with an ESI and APCI interface
(Central Research Laboratory, Hitachi, Ltd., Instrument Division, Hitachi, Ltd.)
Y. Takada, *T. Nabeshima, M. Sakairi, M. Tomioka, T. Mimura, Y. Katoh

2-P-20
Analysis of Antibacterial drugs in meat by Liquid Chromatography/Atmospheric Pressure Ionization-Mass Spectrometry
(Yokogawa Analitical Systems Inc.)
*M.Takino, M.Kaise, T.Yamagami, S.Daishima

2-P-21
Design and development of dual-sector magnet
(ULVAC JAPAN Ltd.) *O.Tsukakoshi , T.Fujita , S.Ogata , S.Shimizu

2-P-22
Multiply-charged Ion Formation in Sonic Spray
(Central Research Laboratory , Hitachi , Ltd.)
*A.Hirabayashi , Y.Hirabayashi , M.Sakairi , H.Koizumi

2-P-23
Experimental studies on resonance enhanced multi-photon ionization time-of -flight mass spectrometry by FEL
(Free Electron Laser Research Institute)
*S.Ogino , K.Awazu , T.Tomimasu

2-P-24
Development of computer program for ion trajectory calculation and display with application to TOF information
(Osaka Univ.) *M.Toyoda , T.Matsuo

2-P-25
New Operation Mode of Ion Source for Sector Type TOF
(Osaka Univ., JAIST) *S.Yamaguchi , M.Toyoda , H.Ito, T.Matsuo , T.Sakurai

2-P-26
Trapping of microparticles at atmospheric pressure
(Osaka Univ.) *M.Yoshida , W.Mo , M.kimura , T.Matsuo

2-P-27
Index Preparation for Heading Parent Parts of CAS Compound Names in NIST MSDB and High Speed Retrieving of the Parts through their indices
(Tsukuba Institute of Science and Technology, Tokyo Kasei Gakuin Tsukuba Women's University)
*Masato NAKAKUBO, Kogoro MAEDA

2-P-28
Hyperthermal Surface Ionization of Organic Molecules: Ratio of the Energy Used Effectively for Ionization to the Kinetic Energy
(Oyama Nat'l college of Tech. , National Inst.for Environ.Studies)
*H.Kishi , T.Fujii

2-P-29
Primary Structure of Poly-phenylene-ether (PPE) Studied by Laser Ionization Tandem Double Focusing Mass Spectrometry
(National Institute of Materials and Chemical Reseach, Sumitomo Chemical Co.,Ltd.)
*K.Ishikawa , T.Nakamura , Y.Koga , E.Yokota , H.Nakajima, K.Ohashi , Y.Obe

2-P-30
Characterzation of Heterofullerenes using Laser Desorption/Ionization Double Focusing Mass Spectroscopy
(National Institute of Materials and Chemical Research , NEDO)
*Nakamura, Takako; Ishikawa, Keiichiro; Yamamoto, Kazuhiro; Ohana, Tsuguyori; Yanase, Etsuya; Yokoi, Hiroyuki; Ryuji, Katoh; Kakudate, Yozo; Koga, Yoshinori; Fujiwara, Shuzo

2-P-31
Development of Laser Time-of-Flight Mass Spectrometer for the Analysis of Composite Films of Magnetic Semiconductor
(Japan Advanced Institute of Science and Technology)
*Toru Sakurai, Yoshihide Seino, Tadaoki Mitani, Masahiro Furusawa Hidenobu Hori

2-P-32
Basic Characteristics of a LC/3DQMS system
(Central Research Laboratory, Hitachi, Ltd.)
*Y.Takada and M.Sakairi

2-P-33
Precise determination of electronic shell structure for gold clusters using mass spectrometry
(Osaka Univ.)
*H. Ito, T. Ichihara, I. Katakuse, X. SUN, T. Matsuo, H. Matsuda

2-P-34
The Catalytic Oxidation of CO with O2 on Gold Supported on TiO2
(Kyoto Institute of Technology, Osaka National Research Institute)
*T. Takao, T. Tode, T. Chijiiwa, Y. Iizuka, S. Arai, S. Tubota, M. Haruta


[Exhibition] 9:00-17:40

[Conference Banquet] 17:50 -



Friday, May 16th, 1997



[Oral Session]


(9:00-10:00)

Chair: M. Takayama
3-O-01
The fragmentation mechanism of 1,2-dimethyl-1-silacyclobutane in EI mass spectrometry
(Nara Women's Univ.)
*Y.Takai , T.Takeuchi , M.Yamamoto

3-O-02
Chiral Molecular Recognition of Crown Ethers Detected by FAB Mass Spectrometry:
The Enantiomer-Labeled Guest Method and the Enantiomer-Labeled Host Method
(ISIR, Osaka Univ., Osaka Inst.Tech., Osaka Women's Univ., Fac.Eng.Sci., Osaka Univ.)
*M.Sawada , Y.Kawai , S.Yodoya , J.Nishida , H.Yamada , Y.Takai , H.Yamaoka , T.Azuma , T.Fujioka , T.Tanaka , K.Hirose , K.Naemura

3-O-03
Quantitative Approach for Chiral FAB Mass Spectrometry by Means of Enantiomer Host Label Method
(Department of Natural Science, Osaka Women's University, MAC, ISIR, Osaka University, Faculty of Engineering, Osaka Institute of Technology)
*Yamaoka, Hiroshi; Kawai, Yorito; Yamada, Hitoshi; Azuma, Tomoko; Fujioka, Tamaki; Tanaka, Toshikazu; Takai, Yoshio; Sawada, Masami


(10:00-11:00)

Chair: H. Yamaoka
3-O-04
Detection of Chiral Amino Acid Discrimination Ability of Cyclodextrins and Cyclofructans
---Application of FABMS EL Guest Method---
(Osaka Municipal Technical Resarch Institute , MAC, ISIR , Osaka Univ., The faculty of Science, Osaka Univ., Osaka Institute of Technology, Department of Biology, Osaka Kyouiku Univ.)
*Shizuma, M.; Yamada, H.; Adachi, H.; Tanaka, T.; Takai, Y.; Miki, D.; Tanaka, T.; Uchiyama, T.; Takeda, T.; Sawada, M.

3-O-05
Metastable decomposition of alkyl trifluoroacetates
(Gunma National College of Technology , Central Glass Co.Ltd.)
*Osamu Sekiguchi , Sou Tajima , Risei Koitabashi, Susumu Tajima and Katsuyoshi Murata

3-O-06
ES-MS Detection of Metal-Ion Complexation Photocontrol Crowned Malachite Green
(Department of Applied Chemistry, Osaka University, Department of Chemistry, Osaka City University, Department of Physics, Osaka University)
*R.ARAKAWA, M.OKAMOTO , G.MATSUBAYASHI , K.KIMURA , M.YOKOYAMA, H.DOE , T.MATSUO


(11:00-12:00)

Chair: M. Sawada
3-O-07
Characterization of cyclic nucleotide isomers by tandem mass spectrometry
(Central Customs Laboratory, Electro-Communications Univ., Sugiyama Women's Univ.)
*T.Hiraki , H.Ando , H.Niwa , M.Ohashi, S.Okuda

3-O-08
Low- and High-energy Collision-induced Dissociation and Metastable Decay of Protonated Methyl Stearate
(Toho Univ., Sankyo Co., Ltd., Jasco Int. Co., Ltd., JEOL Ltd.)
*M.Takayama , T.Kosaka , T.Kinoshita , A.Shibata , K.Tanaka

3-O-09
Structural Analyses of Rare Earth Complexes Using Tandem MS
(Faculty of Science, Chiba University, Chemical Analysis Center, Chiba University)
*H.Tsuruta , K.Yamaguchi , T.Imamoto


(13:00-14:00)
Chair: Y. Itagaki
Plenary Lecture
The Important Role for Mass Spectrometry of Peptides and Proteins in the Post-Genome Era
(Genentech, Inc.) John T. Stults



[Oral Session]


(14:00-15:00)

Chair: K. Hirayama
3-O-10
Mass spectrometry of the polymerase chain reaction product: Diagnosis of single nucleotide base deletion
(Osaka Med.Ctr.BOSHI) *Y. Wada , M. Yamamoto

3-O-11
STRUCTURAL ANALYSIS OF POST-TRANSLATIONAL MODIFICATION OF IMMUNOGLOBULIN Fc FRAGMENT BY MASS SPECTROMETRY
(Faculty of Pharmacy, Meijo University, Faculty of Pharmaceutical Sciences, University of Tokyo, Water Research Institute, GlycoLab, Nakano Vinegar Co. Ltd.)
*Katsuyoshi Masuda , Yoshiki Yamaguchi , Koichi Kato, Yoji Arata , Noriko Takahashi and Ichio Shimada

3-O-12
Structural Characterization of an Antibody against a Porphyrin Derivative
(The Institute of Physical and Chemical Research, Univ.of Tokyo, Univ. of Osaka)
*S.Akashi , K.Kato , T.Torizawa , I.Shimada , T.Imanaka , A.Harada , and K.Takio


(15:00-16:00)

Chair: Y. Wada
3-O-13
Complete Assignment of Digested Peptide of Protein and Characterization of Glycosylation Using LC-ESIIT-MS/MS
(Central research laboratories, Ajinomoto Co., Inc., Tokyo Univ., Water Research Institute)
*R. Yuji, N.Yamada , T.Kashiwagi, U.Tagami , I.Shimada , K.Kato , Y.Arata , K.Hirayama

3-O-14
Femtomole sequencing of proteins and peptides by NanoLC-MS/MS
(Central research laboratories, Ajinomoto Co., Inc.)
*N. Yamada, R. Yuji, T. Kashiwagi, U. Tagami, K.Hirayama

3-O-15
Utilization of FAB in-source Fragmentation for the Structural Analyses of Glycoconjugates
(FRP, The Instit.of Phys. Chem.Res.((RIKEN)), Univ.of Electro-commun., Tokyo Res. Inst.of Nissin Food Products Corp., RIKEN, Fac. of Agricult., Univ. of Tokyo, Mitsubishi Kasei, Inst. of Life Sci.)
*Y. Ohashi , T.Ii , M.Kubota , K.Chino , S.Nunomura , H.Niwa , M.Ohashi, T.Ogawa , Y.Nagai


(16:00-17:00)

Chair: S. Akashi
3-O-16
Analyses of Structures of Protein and Sugar-chain Complexes by the Use of FAB, ESI and MALDI Mass Spectrometry
(Frontier Research Program, The Institute of Physical and Chemical Research(RIKEN), Univ.of Tokyo)
*S.Kurono , K.Yamamoto , T.Irimura , Y.Nagai

3-O-17
Pyridoindole Compounds as New UV MALDI/TOF-MS Matrices for Protein and Oligosaccharide Analyses
(Ehime Univ., Univ. of Buenos Aires)
*H.Nonami, S.Fukui, Y.Fukuyama , and R.Erra-Balsells

3-O-18
Application of Liquid Matrix-Assisted Laser Desorption/Ionization Tandem Mass Spectrometry for the Characterization of the constituents obtained from the Venoms of Spider, Nephila Madagascariencis
(Suntory Institute for Bioorganic Research)
*Y.Itagaki , T.Fujita , M.Hisada , T.Nakajima

[Exhibition] 9:00-14:30


Rev. September 18th., 1998

[The 45th Annual Conference on Mass Spectrometry (Nara)]

[Dr. T. Takeuchi]

[Staffs]

[Department of Chemistry]

Nara Women's Universitry